Large (C>=24) polycyclic aromatic hydrocarbons : chemistry and analysis

Başlık:

Yazar:

Fetzer, John Charles, 1953-

ISBN:

9780471363545

Ek Yazar:

Fetzer, John Charles, 1953-

Yayım Bilgisi:

New York : Wiley-Interscience, c2000.

Fiziksel Tanım:

xvi, 288 p. : ill. ; 24 cm.

Series:

Chemical analysis ; v. 158

Series Title:

Chemical analysis ; v. 158

Konu Terimleri:

Polycyclic aromatic hydrocarbons.

Electronic Access:

Table of Contents http://www.loc.gov/catdir/toc/onix05/00026054.html

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Library	Materyal Türü	Barkod	Yer Numarası	Durum
Searching... Pamukkale Merkez Kütüphanesi	Kitap	0023932	QD341.H9F35 2000	Searching... Unknown

Polycyclic aromatic hydrocarbons (PAHs) are the first type of chemicals that were ever discovered to cause cancer in humans. They are found in cigarette smoke, in barbecued and smoked foods, in automobile and Diesel engine exhaust, fireplace smoke, and many other common things that people are exposed to. Analyzing for PAHs in the environment is important in identifying potential sources of cancer exposure and eliminating these as risks. The smaller PAHs, those of lower than 300 molecular weight, have been the most studied and have also been covered in several books. No books have dealt with the analysis of the larger PAHs. These compounds are not only important for the health concerns, but they are also of current technological and scientific interest.

Author Notes

John C. Fetzer and James D. Winefordner are the authors of Large Polycyclic Aromatic Hydrocarbons: Chemistry and Analysis, published by Wiley.

Preface and Acknowledgments	p. ix
Cumulative Listing of Volumes in Series	p. xi
Chapter 1 Introduction	p. 1
1.1 Introduction and General Discussion	p. 1
1.2 The Smaller Polycyclic Aromatic Hydrocarbons	p. 4
1.3 Structure and Properties	p. 5
1.4 PAH Nomenclature	p. 7
1.5 Carcinogenicity, Mutagenicity, and Other Biological Properties of PAHs	p. 15
1.6 Occurrence of PAHs	p. 17
Chapter 2 The Large PAHs	p. 21
2.1 General Discussion	p. 21
2.2 LPAH Properties	p. 25
2.3 Recent LPAH Syntheses	p. 30
2.4 Theoretical Studies of LPAHs	p. 53
Chapter 3 Ultraviolet/Visible Absorption Spectroscopy	p. 67
3.1 General Characteristics of LPAH Absorbance Spectra	p. 67
3.2 Low-Temperature Absorbance Spectroscopy	p. 82
Chapter 4 Fluorescence Spectroscopy	p. 85
4.1 Introduction	p. 85
4.2 Selective Quenching Techniques	p. 93
4.3 Narrow Line-Width Spectra: Low-Temperature (Shpol'skii) and Other Matrix Methods	p. 95
4.4 Synchronous Scanning Methods	p. 108
4.5 3-Dimensional Fluorescence	p. 112
4.6 Lifetime (Time-Resolved) Methods	p. 116
4.7 Appendix	p. 120
4.8 Phosphorescence Spectroscopy	p. 120
Chapter 5 Infrared Spectroscopy of LPAHs	p. 127
Chapter 6 Mass Spectrometry	p. 131
6.1 Probe and Other Sample Introduction Techniques	p. 131
6.2 Laser Desorption	p. 136
6.3 Selective Ionization Techniques for Isomer Differentiation	p. 144
Chapter 7 Astrophysical Spectroscopy	p. 149
Chapter 8 Chromatography	p. 163
8.1 Chromatographic Sample Fractionation	p. 163
8.2 High-Temperature Gas Chromatography	p. 164
8.3 Thin-Layer Chromatography	p. 171
8.4 High-Performance Liquid Chromatography	p. 172
8.4.1 Normal-Phase HPLC	p. 172
8.4.2 Reversed-Phase HPLC	p. 172
8.4.3 Diode-Array and Other Full-Spectrum HPLC Detectors	p. 183
8.5 Supercritical Fluid Chromatography	p. 188
8.6 Chromatographic Analysis for LPAHs	p. 190
Chapter 9 LPAH Occurrence	p. 205
9.1 Hydrothermal Vent Bitumens and PAH Minerals	p. 205
9.2 Coal Tar and Pyrolytic Pitches	p. 206
9.3 Petroleum and Its Processed Products	p. 212
9.4 Other Combusted Material	p. 218
Chapter 10 Analytical Techniques for Structure Elucidation	p. 227
10.1 X-Ray Crystallography	p. 227
10.2 Annellation Theory	p. 231
10.3 Polarized Light Spectroscopy	p. 239
10.4 NMR Techniques	p. 242
10.5 Photoelectron Spectroscopy	p. 248
10.6 Other Techniques	p. 251
Chapter 11 Sample Prepartion	p. 255
Chapter 12 Comparison of Methodologies	p. 261
12.1 Choosing an Approach for Compositional Analysis	p. 261
12.2 Choosing an Approach for Determining Structure	p. 264
Appendix	p. 267
Index	p. 287

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