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Library | Materyal Türü | Barkod | Yer Numarası | Durum |
|---|---|---|---|---|
Searching... Pamukkale Merkez Kütüphanesi | Kitap | 0023748 | QD79.I5H36 1997 | Searching... Unknown |
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Özet
Özet
This handbook covers the most important instrumental techniques in analytical chemistry, including separation techniques, qualitative and quantitative optical spectroscopic techniques, mass spectrometry, electrochemical techniques, microscopic and surface techniques, and polymer and macromolecular techniques.
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Choice Review
This handbook is a combination of an analytical instrumentation textbook (without the student problem sets), a reference source for analytical applications, and a practical guide to currently available instruments (including information on vendors, level of operator training, service/maintenance, and background readings). Editor Settle (emeritus, Virginia Military Institute) has 28 years of experience teaching analytical chemistry and also coauthored an instrumental methods textbook. The handbook includes a section on sampling techniques and general analytical considerations and covers separation methods, spectroscopic methods, mass spectrometry, electroanalytical techniques, microscopic/surface analysis, and polymer analysis. It contains a substantial glossary and is well referenced throughout. Associated CD-ROM software allows one to efficiently go from either analytical sample parameters or a technique of interest to relevant material on-screen, including references to the appropriate sections of the handbook. The practical and comprehensive aspects of this handbook make it a useful library reference for upper-division undergraduates through postgraduates and faculty, and for private/government laboratories seeking to expand analytical capabilities. J. F. Belliveau; Providence College
Table of Contents
| I Introduction |
| 1 How to Use the Handbook |
| Purpose and Scope |
| Organization |
| Analytical Methodology |
| Technique Selection |
| Summary |
| 2 Sampling and Sample Preparation of Organic Samples |
| Introduction |
| Sampling |
| Sample Transport and Storage |
| Secondary Sampling |
| Sample Preparation |
| Goals and Objectives of Sample Preparation |
| Separation and Preconcentration Techniques in Sample Preparation |
| Types of Samples Encountered |
| Sample Preparation for Solid and Semisolid Samples |
| Sample Size Reduction |
| Drying of Samples |
| Extraction of Soluble Components |
| Extraction of Solid Samples |
| Classical Extraction Technology |
| Modern Technologies for the Extraction of Solids |
| Sample Preparation Methods for Liquid Samples |
| Solvent (or Liquid-Liquid) Extraction |
| Solid-Phase Extraction |
| Column Chromatography as a Sample Preparation Technique |
| The Role of Membranes in Sample Preparation |
| Removal of Particulate Matter |
| Multidimensional Chromatography |
| Derivatization in Chromatography |
| 3 Sample Preparation in Analytical Chemistry (Inorganic Analysis) |
| Classical Chemical Analysis |
| Sampling |
| Sample Drying |
| Sample Weighing |
| Sample Dissolution |
| Extraction, Preconcentration, and Separations |
| Dilution and Matrix Matching |
| Preparation of Standard Solutions |
| Advantages of Sample Preparation |
| Conclusions |
| 4 Quantitative Measurements |
| Limit of Detection, Limit of Quantification, and Sensitivity |
| Calibration |
| Interferences, Contamination, and Loss of Analyte |
| Sampling |
| Verification of Accuracy |
| 5 Managing Laboratory Information |
| Laboratories as Information Producers |
| The Laboratory Testing Loop |
| Properties of Good Information |
| Reliability of Information |
| Relevance of Information |
| Responsiveness |
| Laboratory Information Management System |
| Test Order |
| Sample Collection |
| Sample Check-In |
| Aliquoting and Distribution |
| Measurement |
| Result Entry |
| Result Verification |
| Database Storage |
| Customer Reports |
| Archives |
| Management Reports |
| LIMS Enhancements |
| Conclusions |
| 6 Laboratory Automation |
| What Is Laboratory Automation? Approaches to Laboratory Automation |
| Focused Automation Problems |
| Laboratory-Wide Automation Technology |
| A Laboratory Automation Example |
| Pre-Data-Format Standards |
| Using Industry Standard Data Formats for Exporting Instrument Data |
| Planning for Laboratory Automation |
| Validation |
| II Separation Methods |
| 7 Introduction |
| 8 Gas Chromatography |
| Summary |
| General Uses |
| Common Applications |
| Samples |
| Analysis Time |
| Limitations |
| Complementary Techniques |
| Introduction |
| How It Works |
| Gases |
| Injection Ports and Sample Introduction |
| Columns |
| Detectors |
| Data Acquisition |
| What It Does |
| Analytical Information |
| Qualitative |
| Quantitative |
| Applications |
| Nuts and Bolts |
| Relative Costs |
| Vendors for Instruments and Accessories |
| Required Level of Training |
| Service and Maintenance |
| 9 High-Performance Liquid Chromatography |
| Summary |
| General Uses |
| Common Applications |
| Samples |
| Analysis Time |
| Limitations |
| Complementary or Related Techniques |
| Introduction |
| How It Works |
| Mobile Phase Reservoir |
| Solvent Delivery Systems |
| Sample Introduction Devices |
| Column |
| Detectors |
| Connective Tubing |
| Computer, Integrator or Recorder |
| What It Does |
| Partition Chromatography |
| Adsorption Chromatography |
| Ion Exchange and Ion Chromatography |
| Size Exclusion Chromatography |
| Affinity Chromatography |
| Chiral Chromatography |
| Applications |
| Bioseparations |
